Vype T Peat luble hesizits Substance 29 OCT. i we Oe ly, 1S, 16, on siorke a Pan oqarname Py Core nw. Bones A a neler’ ane. 10.9. Al(oH)s3 oe a os, Ww: Bee. —— Addn. c€ Al (ott), corte, ee eo aon a . Sic a Lose w. Hao, v sat Li. erat AS 13 «hh Roald Bie FEB mo MAR 8 tO 23 = FA aah 4 aa, aie, APRs = * ee 5 2 ee, ‘ck, Bae , itn Lert Be wel. of D0D ex eo. 400enq, ae. APR 1* geben a clbed off, “idee rAd ae? oe _ Per hh teste Selon. HO, cotPaAr « eo = Sh Ata Jin, LS c« - ~ ; a ee oe * =. ke - ‘Gu: ny 2 sp Pe < fe SO eg SEP. a7. See a. Ht, Qk ei Wa cai cA. eee pan te Paredes a Se en Seal is ttc, cacthed OFF 1 SK i, pel e Broo.y Ov tio coBlegd - oct £—- Orvol, of ca. Gaees Lo ce. Vit HCladdlsA, “1 Pe ed oct a ——— ce oh ie (2% Natl 3) ee (A) cece-cted, ain Pe Sich Pv oedina Re ui 20. HCl. RETIRES MOLES Pepa Sap RE gE Az +444. GHP A 1 Az A3 cor~Geed es aget. Aotd, 0. E... auahacadledhke a H,0, N io ae neers oe awed Uti esd. wh e dvskd.. AKL. HOw - (segue t Kinzer a _OcT 144 =" One. rie iF Baa << ee teen ea Oe ade. paper eal =a —— Ate ase ae o. 185g. ] - a Fe UAL e ogo Cae FT praraengpe ar e oft: = ooo Tests ot .4:200. Sola. 2746 Brocefl ae Haga Tre “Tanne Acid = t “ Ngpecte d I- KI cia 4 __ wey 22-3. HPW - . eX iit sg Sea Nw HCE » Ake pore eke Lol oe Ani _ GebeBlene Pb (OP). — Febling tht cas ling, ak. ae ae a tena Te soypatenfaoea Dy im _Pt ciel. ae = Soh Snes bs anos ligt id) a — Bivect ag chive el 4 — £1 ewW —__ teany ipl, Wasck. ve de WL, : ‘ .. Cate. = Gudetewors. ._.. — oi Opa Retebrnee | Ss. - 29 A ocT|24— *Qy. heat 2 | 23,4954 23.4943 Biot hn ee 12d ci 23,4255 OPTICAL, ROTATION . @ > $0. 0/ -p2 O21... Ros, 41-56 157 ss bro oy ! | Fe Tose ap haar ! [| -4225) ———_—_—_— | Metokjeldahls Dee; hake. | Standard » Tog. NV mm 10 ce, Sei Mi lame ta 1M ee | ee | Rage |: 32.8 $L3 32s3 31.0) 30.57 S|ISS.S | prod | Meanit 3 te ended AGT mg. N aloe. SS IGT 2.9 o4,N | | | In jo ce. anh. eta iL =| 207 | | | t i | | | i 1 i 3 L HyAcolysis ocr 2g he. ALLY, C5 ng. wish co. 2N HC] , ot, w. Na 223, Duaadg up & (0 Ve, i | | eS ce, caw Ge BR MNe | i i io a | | & Na 203 id | a | 1A | Ines | So. | 15S) { Ss 0. _ 3,6 Cc 15.70 FG 1-016 = BB =NNbE ag. Cu Nean: (5.8 | = 0.6 aticoas ‘asco 7 | \068 t gz jee ot tS 2,0 omg. o-sboh- _ Reda Svgars t s. lo | | | | Rey? | | | | | | | 30 / 4 { i j j ! q J | | | | | | | | | | | } j ! { i | | | | | | | | | | | | | | | | | | | | i { i i | | | | | | | | | | | | { | | i { { | | | | | | | | | | | | | | | | | | | | | | | | } | i | | | | | | | | | | | | | i == | i j | i | Cake | | | | | | ss.) 29 BO | b 1924 ut. Geta) anoor F3-20Q | 7.4043) 7.40357 7.302% & oiisfs | | 1007 = ROTAT (ON Of | .o2 | OPTICAL Be. + 0.03 0.02 of Wg. 43.05 °F 3.05 | | BD, > > 308 ue. : | | | | | 5 bolas ANY. w. = wet Noch | Oo Ky 43 "Lobe Ls3| 46 | 147 | 149 | | a(Sd¥* : | 5), (Sv¥«L , +306 | | | | | | | | : Miceokyeldabls lees Sample ce “soe (x 1.06) 2,00 | 2.00 | 2,00 | Jo, 10 | & 00 4.44 | (2,22 Lhe t 2 | 2.10 | ce. Yeo hit £0.94 ?) %, 02 | 2-04 | SP | “Lol | | N/ ie Na oH i | a3 | | eee 4,02 | 3.98 j ‘ i | | | | | | Tay | | I ed, | mca cok, 0.0002 4% 5. w | a Roce. iegacivais ALL BR Bde, Gee. wel added , ogi ee at Na 160, oeM(cAT RoTAaT«o M | 0.00 e to. i | 6.3 ol 2. « | Gane, em Oo. [a ¥ Mean: O66 | | | Reo 0496 ~_N | | | | eta | y Ce REG See SY 2o Soe! akon. Bee. ofpse. ashy arr £. ogee. Durned dark, Renrrng! — ot fea Daloeded $faentt Caf combined w 1 | >t | q | | i | | | | | | | a. $. 29 6 | | Aiea N Pets. | | ee | | | | | ocT 20 =] 7. | Gee Rdg. | Core, | M | a poe | Blt | 22.5°) 7949-6) aos | 90.104 | O00 | i | ' i } t i 4 | 0.09% | 0.097 | | — $26} Hi too jeokn nae ge, J 2269 625 %Ior_ tas GE { | 22.8°| 760 | 0,327 | 6.324) e226 | “y ; Zz | a1.¢"| | 0.350 eB O. 4 | 0.2449 | 6244. S650 x19 eb Leeced ak. | i. g les | YoNh, | 4 2.3 dee deen soiere ; ae | eet | 0.210 | , 209 | 109 | NY 4a 107 x. S6¥OxLe 3,07 i | = 1 esti | ha 27 | 167 MZ x sess pe tov 3.31 oe 12,5 mq, DAW 15 | 93. wm lod ce: | 2. : | ¢ | [? “4 = Meany 3.19 — i | | t | | { | | | 1 | | | | | or er Bre es | } { / : { i Minalysts | HY OROLYS iS ocr 22 <— le. 1200 20&y. AOE & tho, © cc. HCt addled. B, & Maa. + aN | OC -tooy leg 42 | Rep + 0.13 41313. Fst tbe | | J, [= + tep® | | | | | |B. t Aa} Comgen, | | | Bx. \+ 0. vf O.090 OLD 30 pa | 12 ce. oats ES 1S, aN uw. Mons, Mec. Than for ad lec, Na $,Pz li. 80 | 23.50 | BEd: (yt) |iq.20 | ht fo | Meant 7s | Hs. | oe | | 27 See! | 72S x Loh x -31% 2 2. BUS. ang, a. = 06 my ees peat, * 333 wf pS os pone i | 268 | te 40 | | Rady: Ssqad ¢S Cale. as 5 lucose | | 3h, 8% H : at aahat, oft NN ant iE 7 = | | 2 Ohede | inl lt, ‘ oc. |S ce. axel 0370. | | | oc. otis gas IS 1141 ]23, 44 vj-3, 6 Wrtifrsdy,re | ryp-3bT ; [14] 24, ee w-O 7 fiat fre vi-T 1/193 [8 by - 1H [1973/8 4 /[193/ 8,9 vl 14, 1/193 /9 u-% Ws 8 )37 ee) psysf—_ |gi-ns ify 8/36 |vr-2 ah naemneneeannnmaiemamemnniaiiamsimmeee Dratted a, ul 35R- Dhak eta ankle lh Sher 3 yee, wane pf recngprpdaad ind d Cae : rtrd - iH ae Ls 12 12 fp flo 6/I 220 Zz 4/00 y , ) edd (6, 270 ec) ag J 7. [+O ce. Ah tuk atk Ce ee 1s. — sili : : = ae ada ate eel ee ale ‘ WEIR, ANNES aT "Salen Aono iad oe 5 ee 2 ve Gon acelaLe co? aletrl £60 ce. pa neat de re ee ee ee — ee Datel tactic Gf hel Le atta poe eet rae Ee Lo eg ee eet. £09 ee. Bot ss ee f So AAOO ce rr ce eel le, - - : ot € . 3O?d ef... ae Eo g ore e ey pA. “Ls. Boece. ed : capac OEE ae shad a OCT 27 — Ppt thee, ap in cn. LOO ce. Ny 9, (oce. 1s, a aan ed co Vpb, cedar rien tho, Mag B cpa Bacerh, o» added G7). Ira ec of of 225 ce, peu. w, LZ. Gansta te a ee ae WORE S 3 ee Ges ao FO cea. siatiadin pd ad, 2.8 _<7.200 26. Questa 6 —— ae Ligh, caShad, a. sea a. H,©, + - an. “or — ee eo va noted Nao Ae. KI@cce. WV AfaoW pane. vot. sf 120 cc. 2 ole ICT 39 ~~ | o COMES AB bee ee 7 Pete. pon fo Pag “29 ave ae. 290 Ma SO ¥ agen Con Ret re. 2k. omar. ons. Fie es le e od — 40 pA ow leo ce. ae. Qh Ped ty Ke - — NOV 8 Different —, 40 Co. athe, anh of (N Hy), SOy Aamerines > fF ___£09, alc NOV 30 = Or Bad. ; ao widsd wlop ec. 33%, i ae cranes 30 v Sastindinndieel ite tohe, gps ey a \ _ cet eo ts 9 ods we “tad ~ gan, call. 2 wy ie - Bon. al AAS ce. Male yi lb abo piel Mase EL Bef po at (@) (A raABy NOV 21— Siberia tok Pinel, wurcksd w. 50. & HoAc, Noy oe. @ aa et aep , th, IBS cc. -w. SWce. : Super alan wa A, —, Sic Ast firm gGreogen Po are Rutan decd. Py. from(C) ( =) / : / Cork “AP, ba ew = 7 ~Oety b - Cad i fe C LLL 4 ¢ ae, N Hey | dale aae4. — oes HzO, ppb. gracushe,, Pevemencia NOV 23 — a: ASA: nip NOV 29 —- po oR! pro 1 — SOW on ant. cr vn hisky eae. ho RB. pi0 2 Whoo, DEC 8 — Cl~ magctive gia n ont, Goto of akc. (inn, CS. acters, warmed § ca, 4o* Dette nc tie Vreld : 1.5%. (Xin gruerund wp, dred" comet wh. nage. A450" he wt: . SK Biucel hegaTi-2 EK: Se cafe ae er Mayum pen cok ; redd & Castanea ape, lydasbyos aka. Corb. Ns Rd Dig il, Ani r ae HCHO : Sprecfie ty att Cot m Hamdaing omer ough W. Ye wh. 49% HCH. aha pec 18 — lesf t. det. cA, NIL-N dD oS SSS. AseLR . 90.1 cc. 36 > 25A, 3) (1, We) added 0.'3 cc. 30% Na NOZ a. O. ce. (OAc added =. RA, RC, Ocor, Gy Rip icil 10 oun, BL. Ww. A,o rouky. Ww. Nao tt a2 made up & ca. S cc, — gree abprsre. N40, ove ag Test. aget Ee; Seca: ee Fyps 1 __Type “hype Oo rer ++ Operas & Reus ot wu, N On %necT. on O pk of SST ost. Acticoa of N, NaoH DEC 24 — oJ ce. acy, + O.t ec. N ne Gi. ck. Gar Cath,» unig | rp. is Specificity aj megnal re, 1: 6, 50, ovd- VAN 2 10°56 = Odes tN NaOH. 1G ec, abe. +30. #0 AUK fo wo ON N.®H, Tinie atl WEH 20 td, es ea, ain, weld wv. Na ~Qnre + QA hf, by Dy cae FAS Be My HCL, GM NaH (x10) 13.40 ae HAL S bu. N= 086~ 14 ~ 447%, ae Ge WY + ae ? 2S , ey 1.26 Sle OI/e-t 985 RS thane ee JAN 1§ — Jeet w. HNO, rp oh hin a can Lave Geom Arete a HtW03 DOs N ce. S.S.36 (1: 200), 0.2 co. Hypo , O-bce. HOA, Abc. cot ASHI, Qo OA cc. = 9 oS: OS ce: 307 NaNO, , Olec. HOAc, Ox Te ee aS y ar, AQA, Ww. H,0, egy wy N Naor LOWE a4 ona hn. Deictiaid 11: olin 2:9 Aye Aihiadi Test @ sagas ro LOY he WW. brs es 00.3 ce. + WwW. N | oth ol nourhy, Ward, Felling s Sola: | — Bod ws NaN, yNaAc > os fo " ee ere e : = Kemer of N HWO, ' a 6 Hl camped a Se Kanrer oh ah. " ae So (42 4). UO,(N03), Gla Lomons pp See. | 9929 DEC | | 2 Ch toute ee 29 ed. Lee 2. DEC DEC 4b | | pS gis cto tba. s\s.s. Cll (2) + abQok 36 mae prada. aid tt eee © = +90 Ol | [a] s+ | | p Micro KvELDA we oop loot 4.70 300° Hus Lt 2.90 - HoknCshen) 9. 9 i i L_ $.05° [| ee | ec hs Wee. ( (obo) 0,223 mg N | 4.46 ia” s 4.57, | ASH | «| “Ov7O | Bhmad ¢ ) NSO pater ot aos we ihanee 0. Ht, | HyDRotysis ARS b Occ. LN HCl / cc, Na2S,03 | 1 / j | | ee > 43\ 1318 2 ahi Co 2 OGL ong. ed. ug. 1.579 Ba. RK een io Nae] 192 | 43sec .9Bl x |, 3t hm 3b Og. Cu = PO | | { Ky. pia Hse, | wong G.25 x ee 8.07SS 8. O75 1 tt aq w. a Nac ( oo ~ ai a iKed . Sa 5 1 } | | i i | ' | } i | i | | i t 8.0742 T9929 | 082 | 72 2.49 | | | | HCI on Ye {2.00 4/, 00 = 1.83 | 2,03 £42. Mean: 215° 1 154 1775 | 1%.63 24-4 is 4s | pee Lee = 5 7 wr¢. ie Na 5.03 ' { %, $9 0. | G4. _| a : fast | a “ 38, + 1. ‘a a. { ; Vag bs “asi | | | i - | | | | | | | | Ae. contd SN CHCIs | | | | + 1 HCla, Yigg | Wel ast { | 2.00 | (SSI | 420 | 2.02 __| | 248 | 3.51 | 17.79 | Fett LADS i — mes | mana] | EFS 19.& ess as” 1ie"/> i | ¥ 3S, 3.5: 3@ DEC 10 Amino N Petus | Hydeplysis goln. (2%) Lee. t Barm . Coc. — (38, 22 267.3 | ooo | 0.99 Packing w. CRL& mn, 298 QyPuy eck 0-323 322 | «BRI SOEE wher 6. ong, ny, N Pap io00c en. i 22.8. ' 0.250 “se 2 24 | 1F0 ¥.FEPmb 4s aa | 2 4.55 22° | o.26$| .26i | 16t BeEe? =O 24. Tomy iit | Jar tod| ce, 112 Slog. “Hyde | Unhydeos)+ Solu. bce. was Rad oy ws bec, Ho. ; 22.5 ©.310 | . 30% | 1.209 STE TO SES aL Cory teh peresoce hy 1sd Cc | a |? | | ) | DEC HroRot ysis ARB, HK. TY CE «ile sae. tS Ce... ode ‘ AMMONIA N ce. Mex HEL (xt20) | BRL RYE | OPT ; E NM 2997, <7 #° 2:00 2.99 Zvo - Noo pein 12.09 15.9% 11.7 16S | cd 2.59 1 S01 Wi. F0 4.04 3.84 £75 370 ay" “ Hej 4.20 Y.09 00 t x Neo 4 4.0% — 2 7s 43.69. | | 2 26 3] i Bs ae | Tin Joe iter. : : Bone lavededs ale f - 17 op | van 125i eo Gh. OBL. a4, EF 0.0 FIN 9: # _ \0,foes’s. 4W3.264i27 3.605 pe if vk | 174 | 6o¥es 43573 : ee | (71933 | 20244 ee aad 4 . | 99733 442% 3 46-3 F It a 76600 | 63b0F | | CacllseOnaNs | Cate HgyO30 Ns i I i bs q ) JAN JAN | JAN > 7 nc 1995 Osh. Cak(s) + ouRab OFF ie HC, I(x Vjo0 NaOH (x to a) Bes isd | At tec a jeoot) HyAroly s( ke = cs. 2.12 14:29 12.00 2. 27 a 36 7, 679Y 7, S519 nN TIF21 7.4020 Loaf 0 Acid Egiewalen’ pe AgNO ce. Noo KCNS(x1. 03) 2% 25x hows a 18, = Hb Iv AgnOs Sow ‘|S c< Miso 424 2.30 1.24 “foto rss w ~t Rv? Zoe hip 2 : , a my Daa, N Na ov, Ne« i. Ss Iver A504 fy X 1:01 Cus DH dH, uuwersed uv, N Na Se. Dhes. longee 15.63 12.92 —, be - xa, awh Sf Ne OF. Titcation 4 Ep. = oF, yer a g, H2o Nis pacard iin, iN 4.ee : 3.68 ae AoiOz ated fe ° mobs od Ach Equiv 2S A Ge Vs ner Mdncy 3, .©% 32 i 7 oi. 36 Alkaline Hydeoly SIS. Nepetition w. 2N Naowl w new A rex tube. AN 12 — . After 2X hes “li 50 Uhes. “ioe 6 hrs. “/100 pts igh eclin 2.00 4.00 2.00 4.00 2.09 G.00 % ie Kio) lo. 24 13.58 14.7% g. 90 Ase |_ 10.20. | 3.43 Hof 2.23] | 2.21 {7G 3,39 $2 370 2S = e Ng N 1.99, 75 $.37,-2- OY, oF Core for BL Q.4 © Se 47 “Ie ae ay , MM ; “4, | ne ae, barren | —“Fotied| =a pag — Lf. qs~ iS. Ge LZ. 03 $.20 S10 42.0 5° 3.90 Ae 2. Ths $ee 3-85 (9 3.29 27 | Mean 0.08 Test fre Phosphocus D ca. 94ln. Ge. we 20. come ttNDs4| (cc. 50, AP | sete fi “tpcead. ee. Ld, by. 20, fo oe Come.) HNO zr added y A> (ity/ Phe Oy Lod . 4 erenlon etartdineg mt | ce x. ; fos . f Crtickiw. vreyerd +| Pog good No ° “best fac Sulphee. | ; : OL tb IS ong, Any » ; eA wu. Na NO3. Pango odor qe _ Dre ong tn Lp oor Y, a HCl, EWa.2d\ (Cas ee when Goll, apn. added. | | : i IN © | FEB 22 Sx. = After Suga ec. RRan fis % GIs Bas 2 Hydcolysis w. HNO, , fe llowed by b. w. H.SOy ce. 89)0, (Jon.s) , Hee. 20%, NaNd, alr, 2ed. HOAC ue? ha Oi. Cah. WS. ocgasignal ahaRe ra, HNO orprrakid ok, tc. 2N H2SOy Ao. Puake up & 22 de. SPTICAK ROTATION O|= 0.03 -0.03 +O)l. iv 0.42 | +4+0.4 . 719) 100 yl = tr 192° D x x Ce GrameP ts Cab iaGece app. * |B 2 On, Grete abe ble QA Oz .e1 | Ol Lar] Gr -.02 RS&g - tole tox +08 to Analysis hee of Seln used (ov 3x - ar mg) Riosolphate 14.90 = K(zo-“S - 4 a 31) - bb ng Copper Ea by: JarD afl O02 bse Eguir.| » Along me cae Lye — ah 19 r Mr. Qo de, O43 2 owe wg hh as “sind - [ o- B+0.0] | 0.5% 40.02 hay + 0109 .92 ls2 fe xj + to2P J, of Ice), Comrcd. on Hr0| Ih & Yee, LD, arta, nf. 2 Be. 20.08 WL, 16.7 he ox bel NG .7S B32 XFS TX .|318 = b.0le-g. Cu + 9, Sg. C3 ee ; of os — edgy. Sugacs ZrO Ys . [ | Lo e Y a JA ae oS ie Acid Hy deolysis = ~] ~ > i) ¢ 7 0.44 9. Fail diad oubok., Oth g. in any . aay. hry Oleg. 1, Made 60ce. W. 420, 6Oc, 2N HC} added, &, 7 Ina. E Fy: pol eS Matte, Fol, Al dearly, PER 44+, 60 cc. more N HCI _ GIGA GUT C. Re ~ Qire. JAN 10 - BEE 2 Doro. Gkid Cob Aad Dy Ke - Gere, JAN 12> He e A rs = | 4 f 25.5. oe Acid H,dcolysis. JAN 14— A - MPW phh, Weed wo. NHC! cory. has} n Pw, ft ok Wb. owed Morn, ane. LR. AP, He) a N OP HA. away YAN 2 LE” Seen. cod cay, 20 decade. a: as ORG N Nich a ok oe Bee y idl. seg Galle) Aeactann pt. of Ba MP2) FED De, oh , (9 We Li Hc a . qoucur- Sithcor ts Coty fa ss Me afe, mond — he he HzSO, ¥ Zee ik rok, -Pb DAc., 4 Oo CA off Kaden sae unas, aff td - os ep NH A. et i ke = Ouaee Ed Sm ona, oo Aruna cap Mw _O..6 S. 36 B_ oct 31 — ark. —— 2 ng added 1b as pelea col ark ot A bt whi oO 2S ce, again PU Hy) 50g. f = =, ducarded . Prri ruopd.cn tre, Sess ¥ een rAdod, acpp Niy), SOy. GuAfed . NOV iss itl, ee M20, e~%P5d «, poured _ sy oa wh fell. H,9.NOV 6- See: fem ep fare gical pe hoi ee andar. ocetenre 5. ArisaA ._ Miedo. Fy Sees stn Risen Bee " si : xs = 36 1B NOV| 8 5 at. koh (+) tacuRot 7.3750, 7.3747 Bere. im thlo ad » 2:29.93 th £8.08. cael «0754 NOV] Lo ; OPTICAL) ROTATION R= 2. O02 ¢€0,06 Los 257 Rig $2.01 196 lucy 4.9 ao =2\it+ 190° ht { j | | | ! i | | | | i Laiaiiiialibianiliiliens ~